data_9007726
_publ_section_title
;
 Tetraammineplatinum(II) bis[pertechnetate(VII)]
;
_journal_name_full               'Acta Crystallographica, Section C'
_journal_page_first              8
_journal_page_last               10
_journal_paper_doi               10.1107/S0108270189004749
_journal_volume                  46
_journal_year                    1990
_chemical_formula_structural     Pt(NH3)4(TcO4)2
_chemical_formula_sum            'N4 O8 Pt Tc2'
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                69.33
_cell_angle_beta                 79.74
_cell_angle_gamma                77.41
_cell_length_a                   5.178
_cell_length_b                   7.725
_cell_length_c                   7.935
_cell_volume                     288.044
_exptl_crystal_density_diffrn    3.315
_[local]_cod_chemical_formula_sum_orig 'Pt Tc2 O8 N4'
_cod_database_code               9007726
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Pt 0.00000 0.00000 0.00000 0.01660
Tc 0.50020 0.33060 0.33600 0.02040
O1 0.38440 0.30940 0.55690 0.03770
O2 0.43460 0.14680 0.28620 0.03580
O3 0.35440 0.53890 0.19370 0.04070
O4 0.83510 0.32200 0.30640 0.03500
N1 0.14690 0.24120 -0.04540 0.02800
N2 0.05780 -0.08940 0.26860 0.02730
